Chairman`s Introduction

Transkript

Chairman's Introduction
When the University of Nigde was founded in 1992, one of the first departments to be established
was the Department of Chemistry under Faculty of Science and letters. From the beginning, the
Department has embodied the University's central mission of excellence in both research and
teaching.
Our current faculty numbers 14, with considerable strength in the core areas of organic, inorganic,
analytical and physical chemistry as well as in interdisciplinary research areas at the boundaries
with biology, physics, soil and materials sciences. Faculty members hold joint appointments with
other departments and many are members of one or more interdisciplinary research institutes,
centers, and committees (for example, TUBITAK (The Scientific and Technological Research
Council of Turkey, and Materials Research Sciences and Engineering Centers).
The Department has been one of the leading positions among Cappadocia regional chemistry
departments. Approximately 65 graduate students are in residence at any one time, and
approximately 10 of graduate students receive Ph.D. and MSc degrees each year. The
undergraduate program is also extremely strong. Some of undergraduates participate in research
projects with the faculty. Very strong interdisciplinary programs are available for interested
students. A particularly popular but demanding program involves chemistry and material science,
engineering, physics and biology. Similar interdisciplinary opportunities exist in the graduate
programs, for example, between Chemistry and mechanical engineering. The projects have been
accomplished so far in the department financially supported by TUBITAK, NATO, State Planning
Organization, European Community, and Agricultural Ministry. Currently, 2 TUBITAK Projects
and one KOSGEB projects have still been continuing besides approximately ten research projects
funded by Nigde University Research Project Units.
The faculty research laboratories of the department are housed in the Science and letters faculty
under teaching laboratories, research laboratories and instrumental analysis laboratories. The
Department operates very good shared-instrumentation facilities that support its research and
teaching missions. The Mass Spectrometry Center features and GS-MS instruments for a wide
range of molecular, cluster, polymer, and biological samples, FAAS is in use for metal
determinations in environmental, pharmaceutical metal containing compounds and industrial
samples, FT- Infrared Spectrometer is located in teaching laboratories with few Ultraviolet
spectrometers. The X-ray Diffraction Laboratory operates state-of-the-art single-crystal and
powder diffract meters with CCD detection and ICP-Ms laboratories located at central research
laboratories of Nigde University. Two HPLC units, one Chromatodrone and JPC chromatography
for polymer science available and are staffed by PhD-level experts.
Aydın Demircan, Chairman
List of Academic Staffs
1. Prof. Dr. Aydın DEMİRCAN (Chair)

Organic Chemistry
2. Prof. Dr. Meysun İbrahim ABDULLAH

Organic Chemistry
3. Assoc. Prof. Dr. Emel BAYOL

Physical Chemistry
4. Assoc. Prof. Dr. İbrahim DEMİR

Inorganic Chemistry
5. Assoc. Prof. Dr. Orhan GEZİCİ

Analytical Chemistry
6. Assoc. Prof. Dr. Mustafa UÇAN

7. Assoc. Prof. Dr. Özlem SARIÖZ

Inorganic Chemistry
8. Assoc. Prof. Dr. Ersen TURAÇ

Physical Chemistry
9. Assist. Prof. Dr. Ali İhsan PEKACAR

Inorganic Chemistry
10. Assist. Prof. Dr. Rifat BATTALOĞLU

Organic Chemistry
11. Assist. Prof. Dr. Selma YILDIRIM UÇAN

Inorganic Chemistry
12. Assist. Prof. Dr. Yavuz SÜRME

13. Assist. Prof. Dr. Demet ÖZKIR

Physical Chemistry
14. Res. Assist. Abdullah Taner BİŞGİN

Dr. Aydın DEMİRCAN
Surname
: Demircan (Dr.)
First Name
: Aydın
Department
: Chemistry
Phone
: +90 388 225 2087 or +90 532 609 2780
E-mail
: [email protected] or [email protected]
Web Address
: http://www.nigde.edu.tr/kimyabolumu/akademik.php?id=498
Educational Background:
BSc: Department of Chemistry, Erciyes University, Kayseri, Turkey, June 1992.
MSc: Faculty of Chemistry, Reading University, Reading, UK, 1995.
Title of Thesis: “An intramolecular free radicalic cycloaddition onto furans”.
PhD: School of Chemistry, Physics and Environmental Sciences, Sussex University, Brighton, UK, 1999.
Title of Thesis: “Cascade reactions involving a furan core”.
Research Field
We have been mainly interested Organic Synthesis with Furan’s compound as well as their methodology
and their cyclisation progress using Intramolecular Diels Alder and free radical cycloadditions. We have
also explored cycloaddition under catalytic condition using Palladium mediated complexes. Currently, our
group produce a smart fertilizing agents like EDDHA-Fe, EDDHA-Zn and EDDHA-Cu for iron, zinc and
copper deficiency for vegetation related to industrial production.
Projects
1. Synthesis and producing smart fertilizing agents, EDDHA-Fe, EDDHA-Cu, and EDDHA-Zn
for metal deficieny in Vegetates, KOSGEB, 2015-FNC-001.
2. Policyclic Ring Construction, using Palladium II acetate and Bu3SnH, supported by DPT(State
Planning Organization) of Turkey, 2002-2004. 3. Intramolecular Diels Alder and Radicalic
cyclization of Furan, thiophene and Pyrrol, Supported by The Scientific & Technological
Research Council of Turkey 2377(103T121) 2004-2006.
4. Domino type reactions of Intramolecular Diels-Alder (IMDA) and Free Radical Reaction to
furan cored compounds; The Scientific & Technological Research Council of Turkey -TBAG(PN:107T831).
5. Establishment of Central Research Laboratory of Nigde University, supported by state planning
organization, DPT. 2010-2013.
6. Theoretical and Practical Training about Spectrometers and Advanced Mycroscopes (SEM);
Supported by EU projects under LLP Programme (PN: 2010-1-TR1-LEO02-14652) 2010-1012)
References
Aydın Demircan, “A Study of Palladium Catalyzed Intra/Intermolecular Cascade Cross Coupling
/ Cyclizations Involving Bicyclopropylidene” Molecules 2014, 19, 6058-6069.
Davit Jishkariani, C. Dennis Hall, Aydin Demircan, Blake J Tomlin, Peter James Steel, and Alan
R. Katritzky, "Push-pull Triazenes Derived from 1-(Benzylideneamino)- and 1-(Sulfonimido)azolylidenes", Journal of Organic Chemistry, 2013, 78, 3349.
M. Karaarslan, E. Gokturk, A. Demircan,‘Thermal Intramolecular Diels-Alder Reaction of
Furan; Synthesis of Nitrogentetracycles, Isobenzofuran And Isobenzothiophene’ J. Chem. Res.,
2007, 2, 117.
A. Demircan, M. Karaarslan and E. Turac, ‘A Facile Synthesis of Heterotricycles From
Furfurylbromoalkenes Using Thermal IMDA Cycloaddition’, Heterocyclic Commun., 206, 8, 233.
A. Demircan, M. Demiralp, Y. Kaplan, M. D. Mat, T. N. Veziroglu,“An experimental and
theoretical study on LaNi5-H2 in two different designated reactors” Int. J. Hydrogen Energ., 30,
1437-1446, (2005).
A. Demircan and P. J. Parsons,"The Synthesis of Fused Ring Systems Utilising the Intramolecular
Addition of Alkenyl Radicals to Furans"Eur. J. Org. Chem., 2003, 9, 1729.
Dr. Meysun İbrahim ABDULLAH
Surname
: Ibrahim Abdullah (Prof. Dr.)
First Name
: Meysun
Department
: Chemistry
Phone
: +90 388 225 4044
E-mail
: [email protected]
Web
Educational Background:
BSc:
Department of Chemistry, Bagdad University, Bagdad, Iraq 1974.
MSc: Faculty of Chemistry, Wales University, Cardiff, UK, 1976.
PhD: Faculty of Chemistry, Wales University, Cardiff, UK, 1981.
Research Field
-
Isolation and Characterization of natural products from Plants
Reaction of Indoles and its derivatives
Toxicological effects of indole’s derivatives
Supercritical fluid extraction
Synthesis of some Erythrina Alkaloids.
References
Özlem Sarıöz, Osman Serindaĝ, Meysun İ. Abdullah” Synthesis and characterization of
Aminophosphines, Bis(amino)phosphine derivatives, and their Molybdenum(0) complexes“
Phosphorus, Sulfur, and Silicon, 184,1785-1795, (2009).
G. Görür, M.I. Abdullah and M.Işık “Insecticidal activity of Thymus, Veronica and Agrimonia’s
essential oils against the Cabbage Aphid, Brevicoyne brassicae” Acta phytopathologica et
Entomologica Hangarica, 43(1), 201-208, (2008).
Ö. Sarıöz, M.İ. Abdullah , “Electrophilic substitution reactions of indole alkaloids with α,βUnsaturated carbonyl compounds in the presence of K10 montmorillonite” ,Russian J.
of Organic Chemistry, ,Vol 42, No 6, 879-882, (2006
Ayten Öztürk , Meysun I. Abdullah; “Toxicological effect of indole and its azo dye derivatives
on some microorganisms under aerobic conditions.”, Science of the Total Environment, 358,
137– 142, (2006).
M. İ. Abdullah, J.C. Young ve D.E. Games; “Supercritical fluid extraction of carboxylic and
fatty acids from Agaricus spp. Mushrooms.” Journal of Agriculture and Food Chemistry, Vol. 42,
No 3, pp. 718-722 , (1994)
M. İ. Abdullah, A.H. Jackson, P.P. Lynch ve K.A. Record; “Electrophilic Substitution on indoles
part 18, Hammet correlations of the coupling of Aryl diazonium tetrafluoroborates with indoles”.
Heterocycles, , Vol. 30, No 1, pp. 317-320, (1990).
M. İ. Abdullah, A.S. Chawla ve A.H. Jackson, “Partial synthesis of 11- oxygenated Erythrina
alkaloids”. J .Chem. Soc. Chem. Comm. 904-906, (1982).
M. İ. Abdullah, A. H. Jackson, et al.; “Studies of Erythrina alkaloids, part lll. GC/MS studies of
alkaloids in the seeds of further fourteen species”.J Ann.Missour. Bot. Gard. 66, pp. 533-540,
(1979).
Ali Gürten, Mustafa Uçan, Meysun I. Abdullah and Ahmet Ayar,“Effect of the temperature and
mobile phase composition on the retention behavior of nitroanilines on ligand-exchange
stationary phase.”Journal of Hazardous Materials, B135,53-57,(2006)
I. Barakat, A. H. Jackson &M. İ. Abdullah, “ Further studies of Erythrina alkaloids” J. of Natural
Products, (Lloydia) 40 (5), pp. 471-475, (1977
Dr. Emel BAYOL
Surname
:Bayol (Dr.)
First Name
:Emel
Department
:Chemistry
Phone
:90 505 7059068
E-mail
:[email protected]
Web Address
Education Background
:
BSc
:Nigde Universty, Art of Science, Depertmant of Chemistry
MSc
: Nigde Universty, Art of Science, Depertmant of Chemistry
PhD
: Nigde Universty, Art of Science, Depertmant of Chemistry
Research Field Description:
Electrochemistry, Corrosion
References
E. Bayol, K. Kayakırılmaz, M. Erbil, The inhibitive effect of hexamethylenetetramine on the acid
corrosion of steel, Materials Chemistry and Physics, 104, (2007) 74–82.
Z. A. Öztürk, R. Battaloğlu, K. Kayakırılmaz, M. Aksoy, E. Bayol, Nutritional status and zınc
levels in serum and hair of university students in Niğde, Turkey, Asian Journal of Chemistry, Vol.
19, No. 6, (2007) 4323-4332.
K. Kayakırılmaz, E. Bayol, H.B. Yılmaz, H.K. Özgün, T. Özbek, D. Topuz, R. Battaloğlu,
Nutritional status and calcium levels in serum and urine of primary hypertensives and
normotensives, Asian Journal of Chemistry, Vol. 20, No. 5, (2008) 3598-3616.
E. Bayol, T. Gürten, A.A. Gürten, M. Erbil, Interactions of some Schiff base compounds with
mild steel surface in hydrochloric acid solution, Materials Chemistry and Physics, 112 (2008)
624-630.
E. Bayol, A.A. Gürten, M. Dursun, K. Kayakırılmaz, Adsorption behavior and inhibition
corrosion effect of sodium carboxymethyl cellulose on corrosion of mild steel in acidic medium,
Acta Physico Chimica Sinica, 24 (2008) 2236-2242.
A.A. Gürten, E. Bayol, K. Kayakırılmaz, M. Erbil, Influence of polyvinylpyrrolidone on rebar
corrosion in sulphate solution, Steel and Composite Structures, 9 (2009) 77-87.
Y. Sürme, A.A. Gürten, E. Bayol, E. Ersoy, Systematic corrosion investigation of various Cu–Sn
alloys electrodeposited on mild steel in acidic solution: Dependence of alloy composition, Journal
of Alloys and Compounds, 485 (2009) 93-103.
Y. Sürme, A.A. Gürten, E. Bayol, Corrosion behavior of mild steel in the presence of scale
inhibitor in sulfuric acid solution, Protection of Metals and Physical Chemistry of Surfaces, 47
(2011) 117-120.
K. Kayakırılmaz, E. Bayol, H.B. Yılmaz, S. Arıoğul, Nutritional status and magnesium levels in
serum and urine of primary hypertensives and normotensives, Asian Journal of Chemistry,
Volume: 23 Issue: 5 (2011) 2175-2180.
D. Özkır, E. Bayol, Inhibition efficiency of benzidine for mild steel in acidic media, Protection of
Metals and Physical Chemistry of Surfaces, Volume: 47, Issue: 4, (2011) 517-527.
D. Özkır, K. Kayakırılmaz, E. Bayol, A.A. Gürten, F. Kandemirli, The inhibition effect of Azure
A on mild steel in 1 M HCl. A complete study: Adsorption, temperature, duration and quantum
chemical aspects, Corrosion Science, 56 (2012) 143–152.
R. Battaloğlu, K. Kayakırılmaz, E. Bayol, Determination of urinary calcium and magnesium
levels by atomic absorption spectrophotometry in hypertensive patients, Asian Journal of
Chemistry, Volume: 24 Issue: 6 (2012) 2369-2372.
D. Özkır, E. Bayol, A.A. Gürten,, Y. Sürme, F. Kandemirli, Effect of hyamine on electrochemical
behaviour of brass alloy in HNO3 solution, Chemical Papers Volume: 67 Issue: 2 (2013) 202212.
Dr. İbrahim DEMİR
Surname
:DEMİR
First Name
:İbrahim
Department
:Chemistry
Phone
:0388 225 4027
E-mail
:[email protected]
Web Address
:-
Education Background :
BSc
:Nigde University, Faculty of Arts & Science, Department of Chemistry
MSc
: Nigde University, Faculty of Arts & Science, Department of Chemistry
PhD
: Nigde University, Faculty of Arts & Science, Department of Chemistry
Inorganic Chemistry,Syntehesis of Metal Complexes and characterization
Dr. Orhan Gezici
Surname
: Gezici
First Name
: Orhan
Title
: Assoc. Prof. Dr.
Department
: Chemistry
Main Field
: Analytical Chemistry
Phone
: +90 388 2254030
E-mail
: [email protected] ; [email protected]
Web Address
: http://nigde.edu.tr/kimyabolumu/akademik.php?id=496
Background
BSc
: Selcuk University, Faculty of Science and Arts, Department of Chemistry (1998-2002)
MSc
: Selcuk University, Institution of Natural and Applied Sciences, Chemistry (2002-2004)
PhD
: Selcuk University, Institution of Natural and Applied Sciences, Chemistry (2004-2010)
Lecturer
: Nigde University, Faculty of Science and Arts, Department of Chemistry (2010 - …)
Postdoc
: ETH Zürich University, Institution for Chemical and Bioengineering (2013-2014)
Research Group: GO-Science Group
Dr. Orhan GEZİCİ
Ahmet Eren ÖZKAN (MSc Student)
İdris GÜVEN (MSc Student)
Seçkin HAYRAT (MSc Student)
Mahmut FİDANCI (MSc Student)
Brief description of the research field:
-
All the aspects of separation and purification methods related with liquid-solid interfaces.
Preparation of new-type adsorbents and stationary phases have been studied in deep. In this
respect, the following topics are within the scope of our research group:
o Adsorption modelling and development of new-type adsorbents
o Development and characterization of new-type of stationary phases for High Performance
Liquid Chromatography (HPLC)
o Particle-packed and monolithic columns
o Surface modification and immobilization process (silica-based materials, magnetite
nanoparticles, cryogels, sporopollenin)
o Protein chromatography
o Frontal analysis and other dynamic methods to derive equilibrium binding data and
isotherm model parameters
o Solid-phase Extraction (SPE)
-
-
o Preparation of new-type of nanofibers by electrospinning process
Easy-to-use analytical methods and/or techniques for determination and characterization purposes
are dealt with.
o Flow-Injection Analysis
o Subtractive FTIR spectroscopy
Application of supramolecules and naturally-occurring biomacromolecules as adsorbent and
stationary phase
o Humic acid; Sporopollenin; Calixarenes
SPE
Adsorption
Chromatography
Separation
Science
Separation
Engineering
Material
Science
New
adsorbents and
stationary
phases
Monolithic
materials
Nanofibers
Magnetite
nanoparticles
Analytics
HPLC
FlowInjection
Analysis
Subtractive FTIR
Maximizing efficiency and information required when minimizing separation-labor!
Selected Publications (Last 5 years)
o
o
o
o
o
o
O. Gezici, M. Bayrakci, Calixarene-engineered surfaces and separation science, Journal of
Inclusion Phenomena and Macrocyclic Chemistry, 83 (2015) 1-18. (Review Article)
I. Perçin, R. Khalaf, B. Brand, M. Morbidelli, O. Gezici, Strong cation-exchange
chromatography of proteins on a sulfoalkylated monolithic cryogel, Journal of
Chromatography A, 1386C (2015) 13-21.
M. Bayrakci, O. Gezici, S. Z. Bas, M. Ozmen, E. Maltas, Novel Humic Acid-Bonded
Magnetite Nanoparticles for Protein Immobilization, Materials Science and Engineering C,
42 (2014) 546–552.
O. Gezici, I. Demir, A. Demircan, N. Ünlü, M. Karaarslan, Subtractive-FTIR
Spectroscopy to Characterize Organic Matter in Lignite Samples from Different Depths,
Spectrochimica Acta A, 96 (2012) 63-69.
O. Gezici, and H. Kara, Towards multimodal HPLC separations on humic acid-bonded
aminopropyl silica: RPLC and LEC behavior, Talanta, 85 (2011) 2405-2410.
O. Gezici, and H. Kara, Towards multimodal HPLC separations on humic acid-bonded
aminopropyl silica: RPLC and HILIC behavior, Talanta, 85 (2011) 1472–1482.
Lectures
General Chemistry
Instrumental Analysis
Modern Chromatographic Techniques
The Chemistry of Humic Substances
Ligand Adsorption
(Undergraduate)
(Undergraduate)
(Undergraduate)
(Graduate)
(Graduate)
(Graduate)
Participated Projects
-
Immobilization of humic acid onto silica and investigating its ion exchanger behavior; S.Ü. BAP
2003-136.
Investigating the Stationary Phase Characteristics of Immobilized Humic Acid by Using Flow
Injection-Chromatographic Methods; PhD Thesis; S.Ü. BAP 082011043.
An investigation of the usability of sporopollenin support in solid-phase extraction and liquid
chromatography; TÜBİTAK 106T090.
Theoretical and practical training on spectrometers and microscobes; Leonardo da Vinci-Mobility
Project; Belgium; Project No: 2010-1-TR1-LEO02-14652.
The usability of humic acid-derived monolithic in protein ion-exchange chromatography; N.Ü.
BAP Projesi, Proje No: FEB-2015/17 BAGEP. 2015 - ...
Synthesis of new-type calixarene-cryogel based columns for protein ion-exchange
chromatography; Project No: 115Z236. TÜBİTAK 1001 Project; 2015 - ...
Referee in
-
Talanta
J. Chromatography A
Anal. Chim. Acta
J. Colloid. Interf. Sci.
-
J. Hazard. Mater.
Sep. Purif. Technol.
Spectrochim. Acta
Desalination
Chemical Engineering Journal
Chemical Engineering Research and Design
Desalination and Water Treatment
Environmental Sci. Technol.
Clean
J. Separation Sci.
Chemistry and Ecology
Turkish Journal of Chemistry
Instrumentation Sci. Technol.
Current Analytical Technol.
and some other journals.
In-situ surface modification of a monolithic cryogel
HPLC separation of three model proteins using the obtained monolithic cryogel column (Application of
SCX chromatography)
Preparation of composite nanofibers
SEM images of composite nanofibers
Preparation of a new-type material for magnetic separation of proteins
Dr. Mustafa UÇAN
Surname
: UÇAN (Dr.)
First Name
: Mustafa
Department
: Chemistry
Phone
: +90 388 225 42 22
E-mail
: [email protected]
Web Address
:
:
BSc
: SelçukUniversity, Faculty of Arts and Sciences, Department of Chemistry
MSc
: Niğde University, Graduate School of Natural and Applied Sciences
PhD
: Niğde University, Graduate School of Natural and Applied Sciences
Research Area:
Solid Phase Extraction of dyes
Preconcentration of dyes by cloud point extraction and solid phase extraction
Publications
Bişgin, A.T., Narin, İ. and Uçan, M., Determination of sunset yellow (E110) in foodstuffs and
pharmaceuticals after separation and preconcentration via solid-phase extraction method, Int. J.
Food Sci. Technol., 50(4), 919-925, 2015.
Bişgin, A.T., Narin, İ., Uçan, M. and Soylak, M., A Comparative Study for Separation,
Preconcentration and Determination of Tartrazine (E 102) in Soft Drink Samples by Two Kinds of
Amberlite Resins, Food Anal. Methods, 8(8), 2141-2149, 2015.
Bişgin, A.T., Narin, İ. and Uçan, M., Comparative column solid-phase extraction procedures for
spectrophotometric determination of E129 (Allura Red) in foodstuffs, pharmaceutical and energy
drink samples, J. AOAC. Int., 98(4), 946-952, 2015.
Yavuz Sürme, A. Taner Bişgin, Mustafa Uçan, İbrahim Narin, Comparison of Preconcentration
and Determination Methods of a Textile Dye by Spectrophotometry: Cloud Point Extraction and
Solid-Phase Extraction, Desalin. Water Treat., 2015.in Press.
Bisgin, A.T., Narin, I, Ucan, M. and Soylak, M., A new cloud point extraction procedure for
determination of trace amount crystal violet in wastewater by UV-Vis. Spectrometry, Oxid.
Commun., 38(1), 232-240, 2015.
Dr. Özlem SARIÖZ
Surname
: Sarıöz (Dr.)
First Name
: Özlem
Department
: Chemistry
Phone
: 903882254050
E-mail
: [email protected]
Web Address
:
BSc
: Department of Chemistry, Faculty of Science and Arts, Erciyes University
MSc
:Department of Chemistry, Graduate School of Natural and Applied Sciences, Nigde
University
PhD
:Department of Chemistry, Graduate School of Natural and Applied Sciences, Nigde
University
We synthesize and characterize aminophosphines, their chalcogen (O, S, Se) derivatives and metal
complexes (Pd, Pt, Mo, Ni, Cu, Co) which may be useful in coordination chemistry, catalytic processes (as
palladium-catalyzed cross-coupling reaction), biological activity studies and applications in electronic
industries. We also investigate as ligands in solvent extraction of metal picrates such as Cu 2+, Ni2+, Co2+,
Cd2+ and Pb2+ from water.
References
Ö. Sarıöz, F. Kandemirli, S. Öznergiz, “Bis(4-methylpiperidinyl)-phenylphosphine and bis(4benzylpiperidinyl)-phenylphosphine: Synthesis, derivatization, molybdenum complexes and DFT
calculations” Polyhedron, 68: 103–111, 2014,
H. Saracoğlu, Ö. Sarioz, S. Öznergiz, “Crystal structure, spectroscopic investigations and
quantum chemical calculational studies of N-diphenylphosphino-4-methylpiperidine sulfide”
Journal of Molecular Structure, 1063: 170–177, 2014,
Ö. Sarıöz, S. Öznergiz, “Aminophosphines Derived From 1-Amino-4-Methylpiperazine:
Synthesis, Oxidation And Complexation Reactions”, Phosphorus, Sulfur, and Silicon and the
Related Elements, 187: 906-913, 2012.
Ö. Sarıöz, Y. Sürme, V. Muradoğlu, “Heavy-metal extraction capability of chalcogenoic
aminophosphines derived from 1-amino-4-methylpiperazine” Chemical Papers, 67 (10) 1345–
1349, 2013.
Dr. Ersen TURAÇ
Surname
: Turaç (Dr.)
First Name
: Ersen
Department
: Chemistry
Phone
: + 90 388 225 40 51
E-mail
: [email protected]
Web Address
: http://www.nigde.edu.tr/kimyabolumu/akademik.php?id=87&ln=en
BSc
: Nigde University
MSc
: Nigde University
PhD
: Nigde University
Conducting Polymer and electropolymerization.
References
Turac, E., Sahmetlioglu, E., Gokturk, E., (2015) Advances in Polymer Technology, “Synthesis of
conducting polymer/zinc sulfide nanocomposite films and investigation of their electrochemical
and morphological properties ”, 34, 1, 21478.
Kumbul, A., Gokturk, E., Turac, E., Sahmetlioglu, E., (2015), Polymers for Advanced
Technologies, "Enzymatic oxidative polymerization of para-imine functionalized phenol catalyzed
by horseradish peroxidase", 26, 1123-1129.
Tuncer, E., Turac, E., (2013) Advances in Polymer Technology, “Synthesis and characterization
of polyaniline /zinc sulphite composite films and investigation of properties”, 32, 4, 21373.
Turac, E., Sahmetlioglu, E., Toppare, L., Yuruk, H., (2011), Journal of Applied Polymer Science,
“Synthesis and characterization of conducting copolymers of quinoxaline derivatives”, 120, 3,
1713-1719.
Turac, E., Sahmetlioglu, E., Toppare, L., Yuruk, H., (2010), Designed Monomers and Polymers,
“Synthesis, characterization and optoelectrochemical properties of poly(2,5-di(thiophen-2-yl)-1(4-(thiophen-3-yl)phenyl)-1H-pyrrole-co-EDOT)”, 13, 3, 261-275.
Turac, E., Sahmetlioglu, E., (2010), Synthetic Metals,“Oxidative polymerization of poly4-[(4phenylazo-phenyimino)-methyl]-phenol catalyzed by horseradish peroxidase”, 160, 169–172.
Dr. Ali İhsan PEKACAR
Surname
: Pekacar (Dr)
First Name
: Ali Ihsan
Department
: Chemistry
Phone
: +90 388 225 4039
E-mail
: [email protected]
Web Address : http://www.nigde.edu.tr/kimyabolumu/akademik.php?id=88
:
BSc
: Selcuk University, 1986, Konya, Turkey
MSc
PhD
-
Synthesis of naphtyl glioxime and their chemical properties
Electrochemical behavior some oxime compounds,
Remove of some metal complexes from industrial waste like Cu, Zn, Pt etc.
Complexes of Ni, Cu and Co with oximes
Interested in macro cyclic compounds
We are also interested in azometyn compounds
References
R. Battaloglu, A. I. Pekacar and Y. Kemal Yildiz, Asian J. Chem. 2012, 24, 2377.
I. Demir, M. Bayrakçı, K. Mutlu and A.I. Pekacar, Acta Chim. Slov., 2008, 55, 120.
I. Demir and A. I. Pekacar, Synth. React.Inorg. Met.-Org. and Nano-Metal Chem., 2005, 35, 825.
S. Yıldırım, A. İ. Pekacar and M. Uçan, Synth. React.Inorg. Met.-Org. Chem., 2003, 33(5), 873.
Dr. Rifat BATTALOĞLU
Surname
: BATTALOGLU (Dr.)
First Name
: Rifat
Department
: Chemistry
Phone
: +90 388 2254052
E-mail
: [email protected]
Web Address
GSM: +90 532 7221390
[email protected]
:
:
BSc
: Selcuk University-Turkey 1991
MSc
: Nigde University-Turkey 1996
PhD
: Nigde University-Turkey 2002
Natural Compounds, Nanofibers from natural compounds, Essential oils, PAH (Polycyclic
Hydrocarbons), Heavy Metals.
Currently, we have developed variety of methods to created nanofibers from natural compounds..
We use electrospinning method. Currently, we are in the process of developing the application in
nanotechonolgy of such natural plant and materials (such endemic plants or honey and pekmez) .
References
M. Gurhan Yalcin and Rifat Battaloglu, Investigation of Heavy Metals Pollution along the
Nigde-Kayseri Road, Turkey, Asian J. Chem., Vol. 19, pp. 2257-2264, 2007
Z.A. Ozturk, Rifat Battaloglu, K. Kayakırılmaz, M.. Aksoy and E. Bayol, Nutritonal status and
zinc levels of serum and hair in university students, Asian J. Chem., Vol. 19, No:6,.4323-433,
2007.
K. Kayakırılmaz, E. Bayol, H. K. Özgün, T. Özbek, D. Topuz, Rifat Battaloğlu, Nutritional Status
and Calcium Levels in Serum and Urine of Primary Hypertensives and Normotensives, Asian J.
Chem., Vol. 20, 3598-3616, 2008.
Dr. Selma YILDIRIM UÇAN
Surname
:UÇAN (Dr.)
First Name
:Selma
Department
: Chemistry
Phone
: +90 388 2254028
E-mail
:[email protected]
:
BSc
: Hacettepe University, 1993, Ankara, TURKEY
MSc
: Nigde University, 1996, Nigde, TURKEY
PhD
: Nigde University, 2002, Nigde, TURKEY
Research Field Description: Synthesis and characterization of Schiff base, Oxime, Glyoxime and
their transition metal complexes.
H
O
CH3
i
NOH
CH3
H
ii
NOH
N
N
L
(a)
(c)
(b)
(d)
HON
H
Dr. Yavuz SÜRME
Surname
: SÜRME (Dr.)
First Name
: Yavuz
Department
: CHEMISTRY
Phone
: +90 533 421 00 80
E-mail
: [email protected]
Web Address
BSc
: Niğde University, Faculty of Arts and Sciences, Department of Chemistry, (2002)
MSc
: Niğde University, Graduate School of Natural and Applied Sciences (2005)
PhD
: Niğde University, Graduate School of Natural and Applied Sciences (2011)
-
Trace element analysis by FAAS.
Cloud point extraction and solid phase extraction on heavy metals and dyes.
Removal, separation and preconcentration of hazardous metal ions from industrial wastewaters.
The main procedure of cloud point extraction
One TUBITAK project is still processing and 5 BAP project are finished.
Selected SCI articles (5 of 18)
Sürme Yavuz, Gürten A. Ali, Kayakırılmaz Kadriye (2013). Electrodeposition, characterization
and long term stability of NiW and NiWZn coatings on copper substrate in alkaline solution.
Metals and Materials International, 19(4), 803-812.
Sarıöz Özlem, Sürme Yavuz, Muradoğlu Vefa (2013). Heavy-metal extraction capability of
chalcogenoic aminophosphines derived from 1-amino-4-methylpiperazine. Chemical Papers, 67
(10), 1345-1349.
Sarıöz Özlem, Sürme Yavuz, Muradoğlu Vefa, Malgaç Burcu (2013). Synthesis and
characterization of triethylammonium 2-(diphenylphosphinoamino)-5-methylbenzenesulfonate
and use of it as a new complexing agent in solvent extraction of Ni (II) ions from water.
Desalination and Water Treatment, 51(28-30), 5409-5413.
Sürme Yavuz, Demirci Onur Burak (2014). Determination of direct violet 51 dye in water based
on its decolorisation by electrochemical treatment. Chemical Papers, 68(11), 1491-1497.
Solid-Phase Extraction, Desalin. Water Treat., 2015.
Dr. Sürme is referee in: Journal of Solid State Electrochemistry, The Journal of Applied
Electrochemistry, Journal of Applied Surface Science, Desalination and Water Treatment, Current
Analytical Chemistry.
Dr. Demet Özkır
Surname
: ÖZKIR (Dr.)
First Name
: Demet
Department
: Chemistry
Phone
: +90 533 620 34 27
E-mail
: [email protected] , [email protected]
Web Address
BSc
: Selcuk University, Faculty of Arts & Sciences, Department of Chemistry (2002).
MSc
: Selcuk University, Graduate School of Natural Sciences, Department of Chemistry
(2005).
PhD
: Nigde University, Graduate School of Natural and Applied Sciences, Department of
Chemistry (2012).
- Material Sciences
- Acidic Corrosion
- Chemical Synthesis including Schiff base and their inhibitor efficiency
- Physical and Electrochemical Properties of the inhibitors in question
- AFM, SEM images of metal and Electrochemical Impedance Spectroscopy
Acid containing solutions are widely used in chemical and several industrial processes such as acid
pickling, acid cleaning, acid descaling and oil well acidizing, which require the use of corrosion inhibitors.
My studies generally focus on the inhibition efficiency of heterocyclic compounds (Schiff base and other
organic compounds) and aim to find application oriented inhibitors. The inhibitor efficiencies of these
compounds are investigated on metal surface in acidic media. These studies were carried out at different
concentrations, temperatures and durations. Electrochemical impedance spectroscopy is a rapid and
convenient method for investigation of protective properties of organic inhibitors on metals. More reliable
results can be obtained by this method. The results are evaluated by using Electrochemical Impedance
Spectroscopy, Linear Polarization Resistance, potentiodynamic polarization, SEM and AFM methods. The
electrochemical experiments are performed with a standard three-electrode cell, consisting of working
electrode, counter electrode, and reference electrode (Ag/AgCl).
References
Demet Özkır and Emel Bayol, “Inhibition efficiency of Benzidine for mild steel in acidic
media” Protection of Metals and Physical Chemistry of Surfaces, 47, 4 (2011) 517–527.
Demet Özkır, Kadriye Kayakırılmaz, Emel Bayol, A. Ali Gürten, Fatma Kandemirli,
“The inhibition effect of Azure A on mild Steel in 1 M HCl. A complete study:
Adsorption, temperature, duration and quantum chemical aspects” Corrosion Science, 56
(2012) 143–152.
Demet Özkır, Emel Bayol, A. Ali Gürten, Yavuz Sürme, Fatma Kandemirli, “Effect of
hyamine on electrochemical behaviour of brass alloy in HNO3 solution” Chemical Papers,
67, 2 (2013) 202–212.
Emin Çadırlı, Mevlüt Şahin, Yavuz Sürme, Demet Özkır, “Thermo-Electrical Properties
in the Pb-Sb Hypereutectic Alloy”, Metals and Materials International, 19, 3 (2013) 465–
472.
Demet Özkır, Emel Bayol, A. Ali Gürten, Yavuz Sürme, “Thermodynamic Study and
Electrochemical Investigation of Calcein as Corrosion Inhibitor for Mild Steel in
Hydrochloric Acid Solution” Journal of the Chilean Chemical Society, 58, 4 (2013) 2158–
2167.
Abdullah Taner Bişgin
Surname
: BİŞGİN
First Name
: ABDULLAH TANER (PhD Student)
Department
: CHEMISTRY
Phone
: +90 388 505 788 00 72
E-mail
: [email protected] , [email protected]
Web Address
: http://nigde.edu.tr/kimyabolumu/akademik.php?id=68
BSc
: Niğde University, Faculty of Arts and Sciences, Department of Chemistry, (2005-2009)
MSc
: ----
PhD
: Niğde University, Graduate School of Natural and Applied Sciences (2009-Continue)
-
-
Currently we have developed various analytical methods including separation, extraction,
purification and preconcentration to determine toxic harmful substances especially heavy metals
and dyes.
Our future researches are synthesis of new artificial or natural resins for determination of heavy
metals by solid-phase extraction method.
We have focused enrichment and separation methods including Cloud Point Extraction and Solidphase Extraction.
References
Bişgin, A.T., Narin, İ. and Uçan, M., Determination of sunset yellow (E110) in foodstuffs and
pharmaceuticals after separation and preconcentration via solid-phase extraction method, Int. J.
Food Sci. Technol., 50(4), 919-925, 2015.
Bişgin, A.T., Narin, İ., Uçan, M. and Soylak, M., A Comparative Study for Separation,
Preconcentration and Determination of Tartrazine (E 102) in Soft Drink Samples by Two Kinds of
Amberlite Resins, Food Anal. Methods, 8(8), 2141-2149, 2015.
Bişgin, A.T., Narin, İ. and Uçan, M., Comparative column solid-phase extraction procedures for
spectrophotometric determination of E129 (Allura Red) in foodstuffs, pharmaceutical and energy
drink samples, J. AOAC. Int., 98(4), 946-952, 2015.
Solid-Phase Extraction, Desalin. Water Treat., 2015.in Press.
Bisgin, A.T., Narin, I, Ucan, M. and Soylak, M., A new cloud point extraction procedure for
determination of trace amount crystal violet in wastewater by UV-Vis. Spectrometry, Oxid.
Commun., 38(1), 232-240, 2015.

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