TURK STANDARDI

TURK STANDARDI
TS EN 590
$ubat 20'14
TS EN 590+41:2010 yerine
tcs
75.160.20
Otomotiv yakrtlan - Dizel (motorin) - Gerekler ve deney y6ntemleri
Automotive fuels - Diesel - Requirements and test methods
Carburants pour automobiles - Carburants
pour moteur
- Exigences et methodes
(gazole)
diesel
d'essai
Kraft stoffe
fU
r Kraftf ah rzeu ge - Dieselkraft stoff
Anforderungen und Prtlfuerfahren
TURK STANDARDLARI ENSTiTUSU
Necatibey Caddesi No.112 Bakanlrklar/ANKARA
TSE DEN izrN ALINI{ADAN SIANDARD|N
&R BOLU|\iUIIAMAI',||
iL I,BAS EDiLEMEZ, QOGALTILAMAZ
ICS 75.160.20
TS EN 590 : 2014-02
TURK STANDARDI
Bu standard, CEN/TC 19 "Gaseous and liquid fuels, lubricants and related products
of petroleum,
synthetic and biological origin - Biyolojik ve sentetik esaslr gaz ve srvr yakrlar, yaglama
yaglal ve
ilgili Urunlei' Teknik Komitesi tarafrndan hazrrlanmrg, cEN tarafrndan 26.01.2013 tarihinde
onaylanmrg ve Turk Standardlan Enstitosu Teknik Kurulu'nu n 13.02.2014 tarihli
toplanttstnda T0rk
Standardt olarak kabul edilerek yayrmrna karar verilmigtir.
Bu standardda kullanllan bazt kelimeler ve/veya ifadeler patent haklanna konu olabitir. Bdyle
patent hakktntn belirlenmesi durumunda TSE sorumlu tutulamaz.
bir
Bu standard yayrnlandrgrnda TS EN 590+41:2010 standardrntn yerini alrr.
cEN uyeleri
srrasryra,Armanya, Avusturya, Bergika, Birregik KraIrk, Burgaristan,
eek cumhuriyeti,
Danimarka, Estonya, Finrandiya, Fransa, Hrrvatlstan, HoIanda, lrranda,lspanya, lsve!, lsvigre,
ltarya,
lzlanda, Krbns, Letonya, Litvanya, Li,ksemburg, Macaristan, Makedonya, Marta, Norveg, poronya,
Portekiz, Romanya, Slovakya, slovenya, Turkiye ve yunanistan'rn milli standard kuruluglandrr.
TS EN
590
2014 slandardr.
Brussels) rzniyle basrlmtslrr.
iiye rllkeleane
EN
590:2013 standardr
ile bircbir aynr otup, Avruf,a
Standardizasyon
Xomitesitinl renue Marnix i7.
B-.tOOO
TS EN 590 : 2014-02
EUROPEAN STANDARD
EN 590
NORME EUROPEENNE
EUROPAISCHE NORM
September 20'13
lcs 75.160.20
Supersedes EN 590:2009+4'1 :201
O
English Version
Automotive fuels - Diesel - Requirements and test methods
Caduranls pour automobiles - Carburants pour moteur
Kraftstoffe fur Kraftfahzeuge - Dieselkraftsloff Anforderungen und Prufverfahren
diesel (gazole) - Exiqences et methodes d'essai
Thas
European Standard was approved by CEN on 26 July 2013.
CEN members are bound to comply with the CEN/CENELEC lntemal Regulations \4rhich slipulale the conditions for giving this European
Slandard the status of a national standard wilhout any alteration. Up-to{ile lists and bibliographacal references coniemiig such nalional
standards may be obtained on applic€tion lo ihe CEN-CENELEC Management Centre or ttany CEN member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by translation
under the respoisibility of a CEN member anto ils own language and notified to the CEN-CENELei vanagem-enttentre hai lhe same
stalus as the official versions.
CEN members are the national standards bodies ofAustria, Belgium, Bulgaria, Croatia, Cyprus, Czech Repubtic, Denmark, Estonaa,
Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, tdland, lreland, ldly, Latvia, Lithuania,
Luxembourg, Malla, Netherlands Norway, Poland, Portugal, Romania, Slovakia, Siov;nia, Spain, Sweden, Switzerland, Tu*ey and United
Kingdom.
E
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITE EUROPEEN DE NORN,IALISATION
EUROPAIScHES KoMITEE FUR NoRMUNc
Management Csntro: AvEnue Marnlx 17, B-IOOO Brussols
O 2013
CEN
All righls of exploitalion in any form and by any means reserved
',lorldwide
Rel No.
for CEN nationat Members.
ruRK STAN0ARDLARININ TEI'F hAKKI
TSE
Y!
ArTTiR. SIANDARDtN BU NUSHASTNTN KiILLAN|M izNr TSE TARAFTNDAN
TURKiYE VAGON SANAYiiA.S.'A VER,LiliSTiF. BAStLt A IARiHi: 15.07.20i5
TSE'DEN iZ'N ALIN[,1ADAN STANDARDIN BiR BOLUiTUiIAMAMt TLTTBAS EDiLEMEZ,
COGALTTLAMAZ.
EN 590:2013 E
TS EN 590 : 2014-02
EN 590:2013 (E)
Contents
Page
Foreword
...........3
2
Normative references
3
Sampling
4
Pump marking
5
5.'t
5.2
5.2.1
5.2.2
5.3
5.4
5.5
5.6
5.7
Other (bio, components...............
Generally applicable requirements and related test
Climate dependent requirements and related test
Precision and dispute
methods.............,
methods.................
Annex A (normative) Details of interJaboratory test
2
programme.........
...............7
...............9
............. 10
.........................
TURK STAND.AROLARININ TILiF HAKKI TSE'YE AiTiiR. STANDARDIN BU NUSIAS]N]N
KULLANItt,I iZNiTSE TARAFINDAN
TURKiYE VAGON SANAYiiA_S_'A VER LMiSTiR. BASTLMA't ARiHi: 15.07.2015
TSE'DEN iziN ALTNMADAN STANDARDTN BiR BoLiM0/rAtvAMl ilfiBAs EDiLHi,4Ez.
QocALTiLAMAZ.
11
TS EN 590 :2014-02
EN 590:2013 (E)
Foreword
This document (EN 590:2013) has been prepared by Technical Committee CEN/TC l9 "Gaseous and liquid
fuels, lubricants and related products of petroleum, synthetic and biological origin", the secretariat of which is
held by NEN.
This European Standard shall be given the status of a national standard, either by publication of an identical
text or by endorsement, at the latest by March 2014, and conflicting national standards shall be withdrawn at
the latest by March 20'14.
Attention is drawn to the possibility that some of the elements of this document may be the subject of patent
rights. CEN land/or CENELEC] shall not be held responsible for identifying any or all such patent rights.
This document supersedes EN 590:2009+A1 :2010.
This document has been prepared under a mandate given to CEN by the European Commission and the
European Free Trade Association [5]
The requirements of the European Fuels Directive 98n1lEC [1], including amendments 2003117|EC 121,
2009/30/EC [3] and 2011/63/EC [4], have been included. Dates are included with all normative test method
references in order to comply with the requirements of the European Commission; with the accompanying
assurance by CEN/TC 19 that any referenced updated versions will always give samilar accuracy and the
same or better precision (see [4]).
Significant technical changes between this European Standard and the previous edition are:
-
lnclusion of the revised EN '14214 FAME specification.
-
Specific requirements concerning the limitation of use of methylcyclopentadienyl manganese tricarbonyl
(MMT) as required by the EC have been incorporated.
-
Addition of the Fuel lgnition Tester (EN 16144) as an alternate test method to the CFR engine test.
-
Addition of Simulated Distillation by gas chromatography (GC), EN ISO 3924, as an alternate test method
to distillation by EN ISO 3405.
-
lntroduction of the improved EDXRF determination technique for low sulfur contents, EN ISO 13032, in
replacement of EN ISO 20847.
Annex A is normative and contains the precision data generated on the test methods, which are the result of
inter-laboratory testing, carried out by working groups of CEN/TC 19. Many of the test methods included in
this standard were the subject of inter-laboratory testing to determine the applicability of the method and its
precision in relation to blends of automotive diesel fuel containing 10 Yo (VN) or higher of different sources of
fatty acid methyl esters (FAME).
According to the CEN-CENELEC lnternal Regulations, the national standards organisations of the following
countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech
Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece,
Hungary, lceland, lreland, ltaly, Latvia, Lithuania, Luxembourg, Malta, Netheriands, Norway, Poland, Portugal,
Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom.
TORK SIANDARDLARIN]N TELIF HAKKI TSE.YE AITTiR STANDARDIN BU NUSHASININ KULLAN M iZNI TSE TARAFINDAN
TURKiYE VAGON SANAYIi A,S.'A VERILIViSTiR. BASiL[,4A TARiHi: 15.07.20]5
TSE'DEN iZiN ALINMAOAN STANDARDIN B1R AO!UMU,'TAMAIVI iLTiBAS EDiLEI\T1EZ, QOGAITILAIVAZ
TS EN 590 : 2014-02
EN 590:2013 (E)
1
Scope
This European Standard specifies requirements and test methods for marketed and delivered automotive
diesel fuel. lt is applicable to automotive diesel fuel for use in diesel engine vehicles designed to run on
automotive diesel fuel containing up to 7 ,0 o/o(Vt\tl Fatty Acid Methyl Ester.
NOTE
For the purposes of this European Standard, the letms
respectively the mass fraction and the volume fraction.
2
"o/o
ltn/ml" and ""k (VM" are used to represent
Normative references
The following documents, in whole or in part, are normatively referenced in this document and are
indispensable for its application. For dated references, only the edition cited applies. For undated references,
the latest edition of the referenced document (including any amendments) applies.
EN 116:'19971), Diesel and domestic heating fuels
prEN 12662:2012'?), Liquid petroleum products
diesel fuels and tatty acid methyl esters
-
-
Determination
Determination
of cold fitter plugging point
of total
contamination in middle distiltates,
-
EN 12916:20061), Petroleum products Determination of aromatic hydrocarbon types in middle d,Sr//afes High perfomance liquid chromatography method with refractive index detection
EN14078:20091), Liquid petroleum products - Determination
middle disti ates - lnfrared spectrometry method
of fatty
acid methyl ester (FAME) content in
EN 14214'.20123), Liquid petroteum products - Fatty acid methyl esters (FAME) for use
heating applications - Requirements and test methods
in dieset engines
and
EN 15'195:20071), Liquid petroteum products - Determination of ignition delay and derived cetane number
(DCN) of middle distillate fuels by combustion in a constant volume chamber
EN 15751:20091), Aulomotive fuels - FaW acid methyt ester (FAME)
Determination of oxidation stability by accelerated oxidation method
fuel and
blends
with diesel fuel -
(DCN) of middle distillate fuels - Fixed range injection period, constant volume combustion chamber method
EN 16329:2013, Diesel and domestic heating fuels - Determination of cold filter ptugging point - Linear cooling
bath method
prEN 16576:2013'?) , Automotive fuets - Detemination of manganese and iron content in middle distillate fuels lnductively coupled plasma optical emission spectrometry (Cp OES) method
EN 2301 5:1994, Petroleum products - Determination of ctoud point (lSO 3O1S:1992)
EN ISO 2160:1998, Petroleum products - Corrosiyeness to copper - Copper strip test (lSO 2160:1998)
EN ISO 2719:2002 , Determination of flash point - pensky-Madens closed cup method (lSO 2719:2002)
1) Under revision.
2) ln preparation.
3) This document is currently impacted by EN 14214:2O12lFptA1:2013.
4
,oaK
sTANDARDLART:'rIN TEL,F HAKK, rsE'yE AirriR. STANDARDTN BU NUSHASTNTN KULLANTM izNi
TURKJYE VAGON SANAY|i A,S.'AVERiLMiSTiN BASII MATARiHi ]507,2015
TsE'DEN iziN ALTNMADAN srANDArtoiN BiR u0t [iMti/] AUAMt iL riBAS EDTLETJEZ. CoGALTiLAMAZ
rsE TARAFTN,AN
TS EN 590 : 2014-02
EN 590:2013 (E)
ENlSO3104:1996, Petroleum products - Transparent and opaque liquids
viscosiy and calculation of dynamic viscosity (tSO 3104:1994)
-
Determination
of
kinematic
EN ISO 3'170:2004, Petroleum liquids - Manuat sampling (lSO 31tO:2004)
EN ISO 317'l:19991), Petroleum tiquids - Automatic pipeline sampling (tSO 31t1:1988)
EN fSO 3405:2011 , Petroleum products - Determination ot distiltation characteistics at atmospheric pressure
(lSO 3405:2011)
EN ISO 3675:1998, Crude petroleum and liquid petroleum products
Hydrometer method (lSO 3675:1998)
EN ISO 3924:2010, Petroleum products
method (lSO 3924:2010)
- Laboratory determination of density -
- Determination of boiling range distibution
EN|SO4259:2006, Petroleum products
-
methods of test (lSO 4259:2006)
EN ISO 4264:20074), Petroleum products
-
Gas chromatography
Determination and apptication of precision data in relation to
- Calculation of
cetane index
vaiable equation (lSO 4264:2007)
EN ISO 5165:19981), Petroleum products - Determination of the ignition
method (lSO 5165:1998)
of
middle-distillate fuels
qual| of
dieseltuets
-
by
the four-
Cetane engine
EN ISO 6245:2002 , Petroleum producls - Determination ofash f/SO 6245:2001)
EN ISO 10370:1995, Petroleum products - Determination of carbon residue - Micro method (tSO 10370:1993)
EN ISO 12156-1:2006, Diesel fuel
- Assessment of /ubrlc ity using the high-frequency reciprocating rig (HFRR)
- Pad 1:Test method (lSO 12156-1:2006)
EN ISO 12185:1996, Crude petroleum and petroleum products - Determination
method (lSO 1 21 85: 1 996)
EN lSO 12205:1996, Petroleum products
(tSO 12205:1995)
-
Determination
of density - Oscitlating U-tube
of the oxidation stabitity of middle-distitlate
EN ISO 12937:200Q, Petroleum products - Determination of water - Coulometric
(tSO 12937:2000)
Kal
fuets
Fischer titration method
EN ISO 13032:2012, Petroleum products - Determination of low concentration of suffur in automotive fuels Energy-dispersive X-ray fluorescence spectrometic method (lSO 1 3032:ZO1 2)
EN ISO 13759:1996, Petroleum products - Determination of alkyl nitrate in diesel fuels
(lSO 13759:1996)
EN ISO 20846:20'1 1, Petroleum products
fluorescence method (lSO 20846:201 1 )
-
-
Spectromatric method
Determination of sulfur content of automotive fuels
EN ISO 20884:201 1, Petroleum products - Determination of sulfur content of aulomotive fuets
dispersive X-ray fluorescence spectrometry (l SO 20A84:201 )
-
-
lJttraviolet
Wavelength-
1
4)
This document is currently impacted by EN tSO 42U:2007 tA1.2013.
lURK SfANDARDLARININTELiF HAK(1]SE'YE AiTTiR STANDARoIN BU NOSHASIN1N KULLANIM izNiTSE TARAFIN
TORKiYE VAGON SANAYI
VERIiMiSTiF I ASILMA TABiHi' 15 07 2015
TSE'DEN lZiN ALINi/ADAN ^1.S.'A
S] ANDARDIN BiR B( LUMU,TAMAVI,LTiaAS ED'LEMEZ. CCGALTITAMAz
5
TS EN 590 :2014-02
EN 590:2013 (E)
3
Sampling
samples shall be taken as described in EN lSo 3170 0r EN tso 3171
and/or in accordance with the
requirements of national standards or regulations for the sampling
of automotive diesel fuel. The national
requirements shall be set out in detail or shall be referred to
by reference in a NationalAnnex to this European
Standard.
ln view of the sensitivity of some of the test methods referred to in this
European Slandard, partacular attention
shall be paid to compliance with any guidance on sampling containers which
is included in the test method
standard.
4
Pump marking
lnformation to be marked on dispensing pumps used for delivering automotive
diesel fuel, and the dimensions
of the mark shall be in accordance with the requirements of natio-nal standards
or regulations for the marking
of pumps for automotave diesel fuel. Such requirements shall be set out in detail
oi shall be referred to by
reference in a National Annex to this European Standard.
Labelling shall be clearly visible, easily legible and displayed at any point where
diesel with metallic additives
is made available to consumers. The label shall coniain: "Contains metallic additives'
in the
language(s)
and shall be laid down in the NationalAnnex to this document.
5
national
Requirements and test methods
5.1 Dyes and markers
The use of dyes or markers js allowed.
5.2 Additives
5.2.1 General
ln order to improve the performance quality, the use of additives is allowed. Suitable fuel
additives without
known harmful side-effects are recommended in the appropriate amount, to help
to avoid deterioration of
driveability and emissions control durability. other technical means with equivalent
effect may also be used.
loTF
developed.
Deposit forming tendency test methods suitable for routine control purposes have
not yet been identified and
5.2.2 Methylcyclopentadienyl manganese tricarbonyl (MMT)
When methylcyclopentadienyl manganese tricarbonyl (MMT) is used, a specific labelling
is required (see also
Clause 4).
MMT is a metallic additive that can be used in diesel. The presence of the
MMT in diesel shall be timited
of manganese per ritre from 'r January 2011. The rimit shal be 2 mg of manganes" p"i ritr" to
tro,
1 January 2014.
6 mg
NoTE
These requirements are subiect to review following an assessment by the European
commission.
5.3 Fafty acid methyt ester (FAME)
Diesel fuel may contain up to 7,0 % (vM ol FAME complying with EN .14214:2012,
in which case the ctimatedependent requiremenls set out in S.4.2 of EN 14214.201i dL not appty.
NOTE
1
A suitabre method for the separation and identification of FAME is given in
EN 14331 [6].
TIJRK STAND.ANDIAF}NIN TEL hAKXI TSE'YE A TTiN. STANSARDIN
AU NUSHAS1NIN Kt]LLAN1]\4 iZNi TSE TARAFINDAN
IURKiYf VAGON SANAYiT A S ,A VER LMiSTiH. Elrls Ua I nn+lt, t5.02 20t5
aSE DEN rzrN ALTNMADAN SIANDAaDtN aiR BOLuv,l, rqr,,rov,
,r t,aeS
gOCar
lJ,L rr,rez.
r rt
eluZ.
TS EN 590
:20i4-02
EN 590:2013 (E)
climate dependent requirements
flyE as a blending component for use in diesel fuel according to this
document are set out in 5 4.3 of P.l
EN 14214:2012. rn" ri""itic grao"s shall be specified on a national
basis
according to locat climatic conditrons and the FAME volume
in ihe diesel fuel.
The finished blend of diesel fuel shall also comply with the climate
dependent requirements set out in 5.6. of
this document.
cold flow additives, when
used in FAME, should be specificafiy matched to the base
diesel fuel and FAME
quality to ensure conect performance.consistent
with the requirJments set out in this European standard. The
choice could result in incompatibility between tne coto ttow'aoJitives
used in the FAME and the diesel fuel.
The choice of
cold flow additive technology should
be a
matter between the fuel blender and the
FAME supplier taking into account the cli;;tic-dependent "ontr"ctr"l
reffiments or the finished dieset fuel.
2 cold ffow requirements for FAME as a blend component in diesel fuel are
set out an Tables 3a and 3b and the
National Annex of EN 14214:2012. in order to
or satrratea monogtycerides in the final EN 590
blend to ensure trouble-free operation. work is "ontror
on-going to ioentirv"onient
a iurtaore test method for saturated monogtyc€rides or
l
a performance test to control this aspect of tow temierjure
NorE
-
,"rirl,
p",f;,f;;e
ln order to improve the oxidation.,stability of FAME, it is strongly
recommended to add oxidation stabitity
.
enhancing additives to FAME at-the production
stage and'beiore storage, providing an oxadation stability
similar to that obtained with 1 ooo,mgikg.or z o-ol-te-rt-uutylJ--hydroxytolrene
(BHT, officially designated by
IUPAC
as 2,6-bis(.1, 1 -dimethytethyt)-4_mJtnytphenog.
The- similar action may be read as providing oxidation
stability performance at least equal to that obtained with
1 000 mg/kg of BHT.
cAUTloN
There is a potential risk of precipitate formation with
oxidation stability enhancing
- low
additives at
temperatures in low aromatic i."iic trei.'6"rtion shoutd
therefore be taken in the
choice of oxidation stability enhancing aoOltives to aiciic
ar"O" feUe.
5.4 Other (bio-) components
Limits for addlng FAME are set for technical reasons.
Limits for
IAME d9 not apply to other (renewabte)
hydrocarbons such as Hvdrokeated veg_etabre oir
cas io Liquid (GTL) or'ei6,n"., io iiqrio (erl)
tHvoi
derived hydrocarbons' since these paraffinic oieser coffinenis
are aflowed in any proportions provided that
the final blend complies with the requirements of
eN sgo. in" ,." ot r"n.*rble feedstock at refineries is also
allowed provided that the final fuel meets the requirem"nt.
oief.iSSO.
NOTE
A draft fuel specification for paraffinic diesel fuel has
been developed [7].
5.5 Generaily appricabre requirements and rerated
test methods
5'5'1 when tested by the methods indicated In Table 1, automotive
diesel fuel shall be in accordance with the
limits specified in Tabre 'r. The test methods risted
in Tabie t have been assessed for apprication to
automotive dieser containing FAME. precision data
from inter-raooratory test programmes are given in
normative Annex A, where these were found to
be different froni tne precision data given in the test
methods
for neat petroleum products.
5'5'2 The limiting value for the carbon residue given in Table '1
is based on product prior to addition of ignition
improver, if used. lf a value exceeding the limit'is
out.in"Jo-n nn-i.t'"d fuel in the market, EN lso 13759 shall
be used as an indicator of the presence of a nitrate-containingcompound. lf an ignition improver is thus
proved present, the rimit varue for the
carbon r"rior" oitt pioo"rct under test cannot be appried.
additives does not exempl the manufacturer tro,
" ih"-requirement of maximum 0,30 o/oThe use of
,*"iing"
rm/m) or
carbon residue prior
to addition of additives
5'5
3
Diesel fuel shall be free from any adulterant or
contaminant that may render the fuel unacceplable for
use in diesel engine vehicles.
NorE
For further information on preventrng contamrnation
by water or sedfient that may occur in the suppty
charn
or for cross-contaminarion. it is advisabre ro
ciiirnn i
r s367_3 lgj respectivery.
"r,,"&
iioiliiii
".'cerna
TI]RKS'ANL,^P',OR\,\-IIII*A"I-'I,YL,AT'IR5.A\NAOIII\6U\L\IIASININKIJLLAN,MZNISF-ANA|INDA\
IIIRK!r r^GoN\AN4,,.^S /ivt t..Mrst,) h.\stt vA,A*,r,, .5r1l,0tr
'..-.
rsE'DEN
iziN ALINMADAT!
sreNoenorN arn a(jLo-^,itj,i,rri,iii"r]iria-["]LEMEz.
cocALrLA[.{Az.
7
TS EN 590 : 2014-02
EN 590:2013 (E)
Table 1
-
Generally applicable requirem6nts and test methods for automotive diesel fuel
Property
Unit
Cetane number
Limits
mtntmum
maximum
51,0
Test method "
(See Clause 2)
D
EN ISO 5165
EN 15195
Cetane index
EN 16144
EN rSO 4264
46,0
Density at 15 "C
kg/m3
Polycyclic aromatic hydrocarbons
Sulfur content
d
820,0
845,0
% (m/ml
8,0
mg/kg
Manganese content r
until 2013- 12-31
from 2014 to 01-Ol onwards
'10,0
mg/l
EN tSO 3675 c
EN tSO 12185
EN 12916
EN rSO 20846 "
EN tSO 20884
EN ISO 13032
prEN 16576
6,0
2,0
Flash point
Above 55,0
s
EN tSO 2719
Carbon residue
(on 10 % distillation residue)
Ash content
o/o
Water content
m9/kg
200
EN
Total contamination
mg/kg
24
EN 12662
Copper strip corrosion
(3 h at 50 :C)
rating
Fatty acid methyl ester (FAME) contenti
%(vM
oxidation stabitty
% (m/m)
l
0,30
(m/m)
0,010
class
Lubricity, corrected wear scar diameter (wsd 1,4) at
60 "c
Viscosity at 40 "C
7,0
pm
mm'/s
(VM rccovercd at 250 'C
Yo (VM recovercd at 350 'C
95 % (UM recovered at
o/o
Yo
o/o
(VM
(VM
'c
rso
12937
h
rso 2160
EN '14078
EN tSO 12205
20
Distillation r'l
EN tSO 6245
EN
1
g/m'
h
EN tSO 10370
EN 15751
460
2,000
EN lso'12156-1
rso 3104
4,500
EN
<65
EN tSO 3405
EN rSO 3924
'
85
360
NoTERequirement5inboldrefertotheEuropeanFuetsolre
2009/30/EC I3l and 2011/63/EU [4].
See also 5.7.4.
See also 5.7.2.
For the purposes of this European Standard, polycyclic aromatic hydrocarbons are defined
as the total aromatic hydrocarbon contenl
less the mono-aromalic hydrocarbon content, both as detemined bt EN 12916.
See also 5.7.3.
See also 5.2.2.
See also 5.5.2 and Annex A.
Further investigation into the total contaminalion test method to improve the prec.ision, particularly
in lhe presence of FA[4E, is being
canied out by CEN.
FAME shall moet tho roquirements of EN 14214, soe
[31.
j
When dieselfuel contains more than 2 %(V/v) FAME, oxidation stability as determined by EN .ls7sl
is lhe requirement.
For the calculation of the cetane index the 10 o/o, 50 % and 90 o/o
recovery poinls are also needed.
ry 4
I
The limits for distirration at 250 "c and 350 'c are induded fordieserfuer in rine with EU
common customs tariff.
EN ISO 3924 gives instrudions to convert to ISO 3405€quivalent data. See also 5_7.5.
8
TURK STANDARDLARININ 'I E LiI iTAKKITS:'YE AITTIR STANDARD
N BU NUSHASININ KULLANIM iZN]
TURKiYE VAGON SANAYiTA.S. A VERiLMiSTaR. aAStL[,4A TARiFi] t5 07 2Oi5
TSE'DEN iZiN ALINMADAN STANOARDiN BiR AOLUMU/TAMAMI ]LTiBAS EDiLEMEZ.
COGALTILAMAZ-
]SE TARAFINDAN
TS EN 590 :2014-02
EN 590:2013 (E)
5.6 Climate dependent requirements and related test methods
5.6.1
For climate-dependent requirements, options are given to allow for seasonal grades to be set
nationally. The options are for temperate climates six CFPP (cold filter ptugging point) gradei and for arctic or
severe winter climates five different classes. Climate-dependent requirements ire given in Table 2 (temperate
climates) and Table 3 (arctic or severe winter climates). When tested by the methods given in Table 2 and
Table 3, automotive diesel fuel shall be in accordance with the limits specified in these tables.
Table 2
Property
-
Climate-related requirements and test methods
Unit
Temperate climates
Limits
Grade
"C, max.
CFPP
-
A
Grade
B
+5
0
Test method
Grade
Grade
c
-5
Grade
Grade
D
E
F
-10
-15
-20
'
(See Clause 2)
EN 116
EN 16329
See also 5
Table 3
7.1
-
climate-related requirements and test methods
Pro perty
Units
CFPP
"C, max.
Cloud point
"C, max.
Density at 15 "C
kg/m",min.
Viscosity at 40
'C
Cetane number EU
e
-
Arctic or severe winter climates
class
class
Limits
class
class
class
0
1
2
3
4
-20
-26
-32
-38
-44
EN'116b
-34
EN '16329
EN 23015
Test method
-10
-'16
-22
800,0
845,0
800,0
800,0
kg/m3, max.
800,0
845,0
840,0
840,0
800,0
840,0
mm2/s, min.
mm2/s, max.
1,500
1,500
1,500
4,000
4,000
4.000
1,400
4,000
't ,200
4.000
51 ,0
51,0
51 .0
51 ,0
m
tntmum
51 .0
a
(See Clause 2)
EN rSO 3675 "
EN ISO 12185
EN lso 3104
EN
tso 5165
d
EN 1 5195
EN 16144
Cetane number
r
Cetane index
Distillation e
mtnrmum
49,0
49,0
48,0
47 ,0
47 ,0
minimum
46,0
46,0
46,0
43,0
43,0
h
recovered at 180 "C
o/o
recovered at 340 "C
o/o
(VlV), max.
1
0,0
10,0
1
0,0
10,0
1
(VM, min.
95,0
95,0
95,0
95,0
95,0
0,0
EN
EN
EN
EN
tSO 5165
15195
16144
ISO 4264
EN tSO 3405
EN rSO 3924
d
I
See also 5.7.1.
See also 5.7.6.
See also 5.7.2.
See also 5.7.4.
Il^:9^T!1i9..-.*h"le
the
!]l-9o_ujEigg--where
the European Fuels Directive 98/70 EC[1] inctuding amendments 2@3nZEC
European Fuels Direclive 98/70 EC[1] incruding amendments 2oo3tiltEC
2009/30/EC [3] and 20'11/63/EU
[4] appties.
l2),
I2l,
2@9/30/EC [3] and 2011/63/EU [4] does not appty.
EU Common Customs Tariff definition of gas oil may not apply to the grades defined for use in arctic or severe
winter climates
For the calculation of the cetane index the
uee atso 5. /.5
io
ok
(vM, 50 % (vM
and go
o/o
(y/y) recovery points are also needed.
T,RK-STANDAROLARININ TELiF HAKKI TSE'YE AiTTIR, STANDARDIN BU NUSHASININ KULLANIM iZNiTSE
TARAFINDAN
TURKryE VAGON SANAYIi A.S_ A VERiLMiSliB. AASttMA IARaHir t 5 07.2015
TSE'DEN iZiN ALINMADAN STANDARDIN BiR AOLLJMU/tAMAMI iLTiBAS EDiLEMEZ,
COGALTILAMAZ
9
TS EN 590 : 2014-02
EN 590:2013 (E)
5'6'2 ln a National Annex to this European Standard, each country shall detail requirements for a summer
and a winter grade and may include (an) intermediate and/or regional grade(s)
which shati be lustitieo by
national meteorological data.
5.7 Precision and dispute
5'7'1
AII test methods referred to in this European Standard inctude a precisaon
statement. ln cases of
dispute' the procedures for resolving the dispute and interpretation of
the results based on tesr method
precision, described in EN ISO 4259. shall be used
5.7.2
ln cases of dispute concerning density, EN ISO 3675
5.7.3
ln cases of dispute concerning sulfur content, either EN
sha be used.
lso 20846 or EN lso 20884
shalt be used.
5'7.4 ln cases of dispute concerning cetane number, EN ISO 5165 shall be used. For the determination of
cetane number alternative methods to those indicated an Table 1 and Table
3 may also be used,-piovided tnat
these methods originate from a recognised method series, and have a valid precision
statement, derived in
accordance with EN lSo 4259, which demonstrates precision at least equal to
that of the referenced method.
The test result, when using an alternative method, shall also have a
demonstrable relationstrip io tire resutt
obtained when using the referenced method.
5.7.5
ln cases of dispute concerning distillation, EN ISO 34OS
5.7.6
ln cases of dispute concerning CFpp, EN
10
1
sha be used.
16 shall be used
TUBI( STANDAADLARININ TELIF I]AKhI TSE YE.AiTTiR SIANDAROIN
_'
iZNi TSE TARAFINDAN
TURhr/tVACO^JSANAYIASAVt q"M,St.n BASrt Vp tAor-r..f BU NOSHASININ KULLANIM
TSE'DEN iziN ALtNMAI)AN SIaNDARDIN BrF BoLitr,,lunalllaur
O,ZittS
"
irria"aiiollaMEz. CocALTlrAMAz.
TS EN 590 : 2014-02
EN 590:2013 (E)
Annex A
(normative)
Details of inter-laboratory test programme
T€bleA:1 presents the precision data obtained in inter-laboratory testing programmes by
CEN/TC 19 [10] and
the El [11], that differ from those of test methods listed in Tabli t anO that at the time
of pubtication of this
European Standard were not yet revised.
NOTE
values:
Ash
The following methods were found to have precision data for 5 %
(vM
F AME btends simitar
to the pubtished
content. EN ISO 6245,
Oxldation stability: EN tSO 12205,
CFPP:
EN 116.
Table A.1
Property
-
Precision data updates
Test method
Unit
5
Viscosity at 40 "C
EN rSO 3104
mm'/s
CEN/TC 19 data for
Yo (VM FAME blend
r= 0,001 1X
R=0,018X
r=2,0
Flash point
EN tSO 2719
Carbon residue
EN tSO '10370
R=3,5
r=0,1430.f5
R=0,2125.Xos
Mrere
r
R
X
is repeatability (EN tSO 4259)
is reproducibitity (EN tSO 4259)
is the mean of two results being compared
TORK STANDAROLARININ
TE!'F HAKKI TSE'YE AiTTiR- STANDARDIN
BU NOSHASININ KULLAN}M iZNiTSE TARAFINDAN
IURKYE VAGON SANAyiiA_S..A VERiLt\,iiSTiR. BASILMA rARiHi: 15.07201t
TSE'DEN iziN ALINMADAN STANDARDIN BiR
aoLtuuteruarvr rrrdei-iolLEMEz.
QocALTTLAMAZ_
11
TS EN 590 :2014-02
EN 590:2013 (E)
Bibliography
t1l
Directive.gErolEc of the European parriament and of the councir
of 13 october .r99g rerating to the
quality of petrol and diesel fuels and amending Council
Directive g3tlZlEEC
12)
Directive 2003/'17lEc of the European parriament and of the councir
of 3 March 2oo3 amending
Directive 98/70/Ec relating to the quality of petrol and djeset fuels
and amending Councit oirective
93t12tEEC
I3l
oirective 2009/30/EC of the European parriament and of the councir
of 23 Aprir 2009 amending
Directive 98/70/Ec as regards the specification of petror, oieseiano gas-oir
and introducing a "
mechanism to monitor and reduce greenhouse gas emissions
and
amending
councir Directive
'1999/32lEC as regards the
specification of fuer ised by inrand walerway vessers and repearing
Directive 93/12lEEC
14)
Directive 201 1/63/EU of 1 June 2011 amending, for th€ purpose
of its adaptation to technicar progress,
Directive 98/70/EC of the European parriamenland ot tne
iouncrt retating to the quarity or peiroi'"J
diesel fuels
tsI
Mandate M/394 - Mandate to cEN on the revision of EN sgo
to increase rhe concentration of FAME
and FAEE to 10o/o vlv, 13 November 2006
t6l
EN 14331:2004, Liquid petroleum products - Separation and
characterisation
esters (FAME) from middre disti ates - Liquid chromatography (Lc)/gas
t7)
cEN/TS 15940, Automotive fuers - paraffinic ctiesel fuel from synthesis
or hydrotreatment Requirements and tes, methods
t8l
CEN/TR 15367-1 , Petroreum products - Guide for good housekeeping
-
pad
tel
CEN/TR 15367-3, petroreum products - Guide tor good housekeeping
-
paft
[10]
of fatty acid methyl
chromatogiapny Gc1';etnoa
12
.
Automotive dieset fuers
3. cross contamination
cEN/TR 15'160, Petroreum and rerate.d products - Appricabirity of
dieset fuet test methods for Fatty
Acid Methyl Esters (FAME) - tnformation and resutts on ,ounO
[11]
1
ioii
tests
El Research Report on lp 398 and EN ISO 10370, under publication,
- avaitable from the Energy
lnstitute, 6 1 New Cavendish Street, London WI G ?AR,
engfanJ
rELiF rrAKKr rsE'yE ArrriR. STATDARDTN
*?I5ililDjlplllllliN
TURKVE vAGoN sANAy iA s.,A vERtMisriR. aAsrL n,te
BU NU.HASTNTN KULLANTM
ririr.,-rr,,.iIor zors
izN,rsE TARAF,NDAN
TSE,DEN iziN ALINMADAN STANDARDjN ain aoL iLIaij,ieLl;.MI.;I
i Ii;As ToiLEMFZ. coGALTILAIJAZ